Gravimetric Analysis of a Soluble Chloride

Objective: To perform gravimetric analysis of money chloride and count on the percent chloride in the experiment. Introduction: Gravimetric analysis is traveling bag on the quantitative isolation of the craved constituentthe analyte of interest, from the exemplification in highly pure form or in some combined form and weighing the isolated constituent. The desired constituent is usually isolated or separated by precipitation. From the masses of sample and boil down, the percentage of the constituent in the passkey sample can be calculated. Precipitation is constituted by organic or inorganic precipitating agents. dickens un wash inorganic precipitating agents are silver nitrate, which is use to return halide ions such as chloride and barium chloride, which is used to precipitate sulphate ion. In these precipitate fight downions, the product is a salt because it is form by reactions between cations and anions. The 3 major requirements for a nigh gravimetric anal ysis are: the reagent will react still with the analyte of interest to form a precipitate, it forms superstar and completely one product with the analyte and the analyte precipitates quantitatively from dissolving agent.

In aqueous solution silver ion undergoes the following reactions with chloride: Ag+ (aq) + Cl- (aq) ? AgCl (s) Experimental Methods: Three crucibles were well washed with soap and water. The cleaned crucibles were whence mounted to a tense flask, and 2 mL of concentrated nitric corrosive were allowed to soak. The acid was deadened via a gentle vacuum. This was repeated 2 more times. The crucibles were then rinsed with deionized wa! ter. Three portions (0.316g, 0.305g, and 0.298g) of dried chloride sample were dissolved in 3 separate 400 mL beakers in cl mL of deionized water and 1 mL of concentrated nitric acid. The three chloride solutions were then heated, and silver nitrate solution was added in 5 mL increments (while stirring vigorously) until precipitation of the silver chloride was complete. individually beaker was then...If you compulsion to get a full essay, order it on our website: BestEssayCheap.com

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